The X-raysingle crystal data setwas measured on a Rigaku Mercury CCD X-ray diffractometer equipped with a graphite monochromated Mo-Karadiation (l = 71073 Å) through an wscan By means of CrystalClearsoftware， the data was reducedand empirical absorption was corrected[[i]]The single crystal structure was solved by using direct methods in virtueof the Siemens SHELXTL TM Version 5 package of crystallographic software[[ii]]The hydrogen atoms were symmetrically generated and allowed to ride on the parentatoms， while the non-hydrogen atoms were yielded on the sites of the differenceFourier All the hydrogen atoms were used to the structural factorcalculations but were not The single crystal structure of the titlecompound was refined via a full-matrix least-square refinement of F All the non-hydrogen atomswere refined Some crystal data and structural analysis detailswere listed in Table Selected important bond distances and bond angles were shownin Table 在X raysingle晶体数据setwas上配备了石墨的理学水星的CCD X-射线衍射仪测定通过wscan技术单色Mo - Karadiation （ λ= 71073 Å ） 。通过CrystalClearsoftware手段，数据是reducedand经验吸收校正[[i ] 。单晶结构解决了使用中凭借西门子SHELXTL TM版本5封装的晶体学软件的直接方法[ [ II ]的氢原子被对称地生成，并使其骑在parentatoms ，而非氢原子分别得到的differenceFourier地图的网站。所有的氢原子被用来构造factorcalculations但没有细化。该titlecompound的单晶结构通过F2的全矩阵最小二乘精化被提炼。所有的非氢atomswere精制各向异性。一些晶体数据和结构分析detailswere列于表1 。选取重要的键长和键角分别shownin表2。这样吗？帮你查的。
